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Pentaerythritol analysis by GC

Posted: Thu Sep 02, 2010 2:44 pm
by Jan Lorier
I need to analyse some sample for Pentaerythritol content (ppm)
My idea was to do this by gc using derivatisationby silylation

Anyone some good ideas how??

Thanks,

Jan

Posted: Wed Sep 22, 2010 4:46 pm
by Phycal
Acetylate? You can do this with Acetic anhydride and 1-methylimdazole as the catalyst.