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How to turn off Split mode in 5890 series II plus

Posted: Sun Aug 15, 2010 9:35 am
by vliu
Hi, could someone please advise me how to switch from split mode to a splitless mode in 5890 using the panel buttons. Do I need to change the liner if it doesn't state in my method which liner to use.

If I switch to splitless mode then how do I check the purge flow??

Thank you.

Posted: Sun Aug 15, 2010 10:58 pm
by aldehyde
Do you have EPC control? Do you operate from the front panel or computer?

There is a purge button on the front panel, you turn the purge off at the beginning of the run, inject, and then turn the purge on at some point to sweep sample remaining in the inlet out the split vent. You may need to press the button several times to configure the timing, but the time you turn it on is dependent on the method. Probably after 0.5 or 1 minutes.

If you use chemstation you can configure this in the method.

Measure your purge flow using a flow meter attached to the split vent port on the front of the GC.

As far as the liner goes a "straight through" liner with glass wool works for most applications. If you have especially active compounds, or a wide boiling point range skip the wool. Taper or not is determined by the method. What solvent is your sample dissolved in? There are calculators available that tell you the expansion volume of your injection so you can be sure you're not exceeding the volume of the liner.

Here is a page on Agilent's site that talks about the reasoning for some liner features:
http://www.chem.agilent.com/en-us/produ ... 18299.aspx

Here is a list of liner part numbers: http://www.chem.agilent.com/en-US/Produ ... icing.aspx

5181-3316 is probably what you want.

Posted: Tue Aug 17, 2010 7:59 am
by vliu
Thank you so much for the info.

Posted: Tue Aug 17, 2010 11:41 am
by aldehyde
sure, let us know if you have more questions.