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Better peak shape

Posted: Thu Jul 15, 2021 11:26 am
by jsdelcarmen
Good day! I ran a standard of carbon disulfide in isooctane with HP-5MS and I observed that my peak is tailing/broadening. Any suggestion on how I can achieve a better peak shape? Thank you!

Re: Better peak shape

Posted: Thu Jul 22, 2021 9:41 pm
by James_Ball
Good day! I ran a standard of carbon disulfide in isooctane with HP-5MS and I observed that my peak is tailing/broadening. Any suggestion on how I can achieve a better peak shape? Thank you!
What type if inlet are you using?

What inlet liners?

Injection volume and is it splitless or split?

Inlet temperature and initial oven temperature?