Advertisement

Any tricks to remove a stuck liner insert?

Discussions about GC and other "gas phase" separation techniques.

6 posts Page 1 of 1
This splitless glass insert column was probably since the day 1 on a HP 5890 GC. I used a knife to cut off the o-ring as much as possible, but the it won't move at all.

How to remove a stuck insert without permanently destruct it? Anyboy has ideas?

I'd remove the column and the inlet nut/gold seal (in the column compartment). Then I'd use one of the 1/4 inch stainless steel liners (provided with the GC) and tap downwards with a small hammer. Sure the old liner will probably break, but just wash out any particles with a solvent like methanol, and brush clean, rinse again, and reinstall with new liner, new gold seal and washer, etc.

I find that a sharp cork borer ( usually nickel-coated brass ) will slide over the outside of the liner and cut the O-ring from the insert all the way down to the O-Ring seat ( being brass, the seat isn't damaged ).

I also will remove the column nut and seal, but force the insert UP - as the viton/silicone becomes so hard after prolonged use at high temperatures it's difficult to push any residual O-Ring past the lower seat. . I tap out the insert using a short piece of plastic rod ( such as packs of 10 1/4" Swagelok ferrules come on ).

If I even use a hammer on glass, I use a small piece of hard wood or plastic to dissipate shock - never broken an insert yet.

Bruce Hamilton

Thank you, Bruce and Consumer Products Guy for the quick reply!
I will see if I can get it off.

Hey Bruce Hamilton is from New Zealand: no wonder he accesses this from "down under" !!!

Try heating the inlet up to normal working temp and remove the liner when it is still hot.....be careful.

GCguy[/img]
GCguy
6 posts Page 1 of 1

Who is online

In total there are 21 users online :: 0 registered, 0 hidden and 21 guests (based on users active over the past 5 minutes)
Most users ever online was 4374 on Fri Oct 03, 2025 12:41 am

Users browsing this forum: No registered users and 21 guests

Latest Blog Posts from Separation Science

Separation Science offers free learning from the experts covering methods, applications, webinars, eSeminars, videos, tutorials for users of liquid chromatography, gas chromatography, mass spectrometry, sample preparation and related analytical techniques.

Subscribe to our eNewsletter with daily, weekly or monthly updates: Food & Beverage, Environmental, (Bio)Pharmaceutical, Bioclinical, Liquid Chromatography, Gas Chromatography and Mass Spectrometry.

Liquid Chromatography

Gas Chromatography

Mass Spectrometry