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HED Supply Difficulty

Discussions about GC-MS, LC-MS, LC-FTIR, and other "coupled" analytical techniques.

47 posts Page 4 of 4
This is actually really crazy because we're having that same problem but on a different 5975. Unfortunately we haven't fixed it yet. I tried cleaning the HED but that didn't seem to do anything. I've never really come across this problem before so troubleshooting it is a little tricky. At first I thought there might be some metal touching metal but I couldn't see any discrepancies in the detector. There didn't appear to be any dust anywhere either. I can't believe we're still having the same problems as each other...
Yeah! I believe so... By the way, our air components abundances were reducing gradually. But still, I'm having a lot of peaks across the scan from 10 to 700 m/z. Have you try to check the pressure inside the ion source chamber?

Thanks.
What do you have the threshold set to in your tune? Normally it is run about 50-100 counts. If you have the threshold set to 0-10 counts you could easily get those 800 peaks across the scan. The lowest I have ever been able to run my threshold was 10 and that was after it had been running for a week and I had reduced the multiplier voltage as low as I could without loosing sensitivity.

James,

I'll be checking on regarding the threshold set on the GC-MS. Later, I'll power on the MS because it was turned off (as instructed by the service engineers). I'll get back to you on this...

Thanks.
Guys!

We've fixed the problem!!! The only thing we did was to clean the EM Horn and replaced the vent valve and calibration valve o-rings. I noticed it because once I ran tunes using PFTBA, the water and air components increases overtime.

Thanks for helping me out.
47 posts Page 4 of 4

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