GC-FID one peak present(solvent only or coelution?) Ver 3.1

[Kashew]

I'm going to try tweaking that process that gave me those insignificant, tiny peaks...see if that helps me get some actual separation between the compounds.

Also, I'm using this column:

http://www.sigmaaldrich.com/catalog/Pro ... KEY&F=SPEC

If anyone was wondering.(I think it's in the old thread I link in the OP but no harm in linking it again)

[Bigbear]

Those peaks come out quite fast. Your flow and ramp rates may be a little high.
I would suggest that you do an injection starting at 40 for one min. Then ramp the oven at 10- 12 degrees /min. just to see if you get separation. When you see the correct number of peaks you can then take steps to shorten the run time.