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- Posts: 325
- Joined: Fri Apr 08, 2011 6:15 am

What should know the lab? Everything.
What should know the docent? Which book is described
What should know the professor? In what room sits docent
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Off-topic conversations and chit-chat.
As a newer trained analytical chemist (MS degree) I can attest that you are correct about your final statement. I've met a whole bunch of extremely great analytical chemists and elite technical experts as Peter Apps stated. The one thing that they have in common is that they are all either retired or close to retirement. I found my education in graduate school rather lacking as the instructors were too busy teaching 10 sections of general chemistry and put off the advanced analytical courses. As a result I was not able to take a graduate chromatography. I got in analytical spectroscopy and mass spectrometry as well as 2 semesters of graduate Organic sythesis (worthless to my field). These were the only courses offered. The analytical classes were only offered every other year.Things have changed. I now get copious school visits from students bearing stuff they've made, and accompanied by teachers keen to prove they've made the right thing. It's a good step. I blame CSI for much of it.
At the moment I'm not totally convinced analytical chemistry should be taught in isolation. I haven't been impressed by the level of knowledge of the few I've met who've trained as pure analytical chemists. But perhaps I've been unlucky.
Just saw this.And for computing power. We got to punch data onto punchcards and run the program (in FORTRAN IV) at the computer center - which had the computer in this nice, large air conditioned room because of the heat it generated. Cards in the hopper - printout on greenbar paper - and if it did not work, you took the paper and figured out what was missing in the middle.
You are a bit misstaken in the FTIR stuff.. In the mid 70's I was using an FTIR made by DIGILAB which used a Data General NOVA computer with front pannel switches that had to be booted off of punched tape! Of course that was on a CO-OP job (worked half the year and in school the other half in a 5 year BS program) working for the Army at a research center. Besides the FT calculation and signal averaging it could subtract spectra!!! I have NO idea what it cost back then, but in today's dollars I suspect quite a LOT!!! It was probably one of the first commercial instruments.From when I was in school (1970's) to to day all of the equipment I had my hands on has become obsolete. The underlying theory remains the same. Chromatography is all about partitioning - to this day. Capillary has changed chromatography dramatically - and made the interface with a mass spec practial. IR - the bands are made by the same stretches, wiggles, and wags in the molecule -- and at the same wave number. The FTIR was never heard of - the laser did not exist and the computations were far beyond what we could do.
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