Chromatography Forum

Chromatography Forum is a public discussion group where you can post questions, news, or messages of interest to chromatographers everywhere, but you must be registered to participate (registration is FREE). If you are a registered user, please log in.
http://www.chromforum.org/

poor peak shape when analysing FAMEs on GC-FID

http://www.chromforum.org/viewtopic.php?t=16157

Page 2 of 2

Re: poor peak shape when analysing FAMEs on GC-FID

Posted: Fri Apr 15, 2011 1:30 am
by EUROFINS
Another thing with this type of methylation is the resaponification of short chain FAME in time. You can prevent this by neutralizing the NaOH with NaHSO4.H2O. See ISO http://www.iso.org/iso/iso_catalogue/ca ... mber=34610 or http://www.iso.org/iso/iso_catalogue/ca ... mber=43172 or http://www.iso.org/iso/iso_catalogue/ca ... mber=28897

Interesting link: METHYLATION OF FATTY ACIDS – A BEGINNER'S GUIDE
All times are UTC
Page 2 of 2
Powered by phpBB® Forum Software © phpBB Limited
https://www.phpbb.com/