Posted: Fri Aug 20, 2010 6:49 am
Syringe Temperature should be 10°C + Oven Temperature of the autosampler.
In autosampler method:
- try to add a sample prefilll step (3 repetition) for sample homogenization before injection
- Be sure to have inserted an appropriate post-purge step for cleaning syringe by nitrogen flush.
Does it help?
In autosampler method:
- try to add a sample prefilll step (3 repetition) for sample homogenization before injection
- Be sure to have inserted an appropriate post-purge step for cleaning syringe by nitrogen flush.
Does it help?