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Correct way to measure FID flow rates

Discussions about GC and other "gas phase" separation techniques.

3 posts Page 1 of 1
What is the correct way to measure FID flow rates? I have a digital flow meter with a button to change the gas being measured which accounts for difference in density. Our FID calls for a H2 flow rate of 40 mL/min, and air of 450 mL/min, and I have been measuring it using the meter set to the appropriate gas, which presumably gives a "adjusted" flow rate. Is this correct, or should I just use the "air" setting for both, that way the ratio is a true volumetric ratio?

If you really care that much: measure each gas with the flow meter set for that type of gas.

If the flow meter really is calibrated for different gasses it must be correcting for more than just density (thermal conductivity for a start I would think). I'm with CPG; if it has a setting for each gas go ahead and use them.

The only reason that I can think of for correcting for only density is if the readout is in mass per unit time. Which would be strange. What make and model is it ?

Peter
Peter Apps
3 posts Page 1 of 1

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