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Tuning

Discussions about GC-MS, LC-MS, LC-FTIR, and other "coupled" analytical techniques.

3 posts Page 1 of 1
Hi all,
I'm very frustrated on tuning my GC/MS. The target mass of 75 relative to mass 95 always failed off the range. I tried to do autotune and bfb tune but in vain. I really don'n know what to do next. Please advice.
Thanks all, Spectro.

Spectro,

Post your tune, post your BFB maximum spectrum or your tune report. Without more data no one can really help you.

Best regards.

I have had problems with 75 creeping up near 95 and autotune and bfbtune not being able to bring the tune within limits. When this happens i generally clean the instrument and that solves the problem.

There was one instrument a few years ago that would not tune with the automated tune process regardless of which one you used. I wound up running a BFBtune and then adjusting it by hand to get it to tune. I just maximized everything using the ramp function and then went back and adjusted it to bring it back in line with what it should be. I fought it like this for a few months and then it just started working fine. I suspect it was either the repeller or a lens that was not sanded properly and eventually it got whatever was wrong worked out as it was cleaned, but who knows! These beasts are fickle sometimes.
3 posts Page 1 of 1

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