Alkyl lead by GC-MS

[JonKlar]

Hey guys

I've recently been tasked with creating a method for alkyl lead by GCMS. I can't seem to find any ms specific methods online and was wondering if anyone has done anything like this? If anyone does this I would be very interested in your method parameters and column of choice.

I will continue to work on this but am very greatful for any input you might have!

Thanks again,
Jon

[Yama001]

Our folks have done Tetraethyl and Tetramethyl lead under the EPA 8270 method.

[JonKlar]

Great news, thats where I planned on starting. Do you know of a vendor for reference standards?

[Yama001]

It looks like our BNA crew is getting them from Accustandard.

[mckrause]

It is fall-off-a-log easy using USEPA 8260 protocol. Switch to SIM once you have conditions established and you'll have mid-ppt sensitivity.

[JonKlar]

This is great. Thanks so much everyone!

Jon

[LALman]

It is fall-off-a-log easy using USEPA 8260 protocol. Switch to SIM once you have conditions established and you'll have mid-ppt sensitivity.

Please give details.