Advertisement

Purge & Trap is not purging!

Discussions about sample preparation: extraction, cleanup, derivatization, etc.

2 posts Page 1 of 1
Dear chemists!

I hope you can help me with a trouble on my Eclipse 4760 P&T (coupled with an 4551A autosampler). Basically it's not doing one of the two things it's supposed to do, is not purging.

After a long period of inactivity (one year) the instrument does not produce bubbling in the sparger. The pressure and the flow are ok (Flow 40 ml/min and System Pressure 20 psi), leak tests are succesfully passed, all the screw are tested and there is no bubbling after soap-testing all the screw, Helium pressure from the tank is ok. It seems that the only thing non ok is the bubbling in the sparger :roll: . I also tried to change the sparger.

I am completely new in the field of the Purge and Trap system, so hope you can help me and forgive my ignorance.

btw there is no techincal support here in Italy from OI analytical

Thank you all!
I don't know the Eclipse. Could there be a valve that isn't switching correctly?

Somewhere between your cylinder and sparge tube, there's a problem. I would want to try to disconnect the tubing at points along the relevant flow path one at a time to try and isolate the problem. If it can be done safely, I'd also try using a multimeter to make sure the valve is getting a signal to switch at the right time.
2 posts Page 1 of 1

Who is online

In total there is 1 user online :: 0 registered, 0 hidden and 1 guest (based on users active over the past 5 minutes)
Most users ever online was 1117 on Mon Jan 31, 2022 2:50 pm

Users browsing this forum: No registered users and 1 guest

Latest Blog Posts from Separation Science

Separation Science offers free learning from the experts covering methods, applications, webinars, eSeminars, videos, tutorials for users of liquid chromatography, gas chromatography, mass spectrometry, sample preparation and related analytical techniques.

Subscribe to our eNewsletter with daily, weekly or monthly updates: Food & Beverage, Environmental, (Bio)Pharmaceutical, Bioclinical, Liquid Chromatography, Gas Chromatography and Mass Spectrometry.

Liquid Chromatography

Gas Chromatography

Mass Spectrometry