H2O2 analysis

[Chandresh K. Soni]

Hi
My Problem is to Analyse the H2O2 Content in a Solid Comp. on GC
Is it possible on FID or on TCD . If yes Then Which Column i Preffered.
pls suggest me.

[MikeD]

Not possible by FID and while I would never say never to GC-TCD this article below describes a few HPLC options involving oxidation of substances like triphenylphosphine or formation of iron (III) or titanium (IV) complexes.

http://www.rsc.org/delivery/_ArticleLin ... i=a806432f