Transferring Loop injection to Syringe injection with split

[Raphael Divekar]

I have a vendor's GC headspace method for determination of impurities and have to adopt in my laboratory. The method uses a loop injection method while we a syringe injection method with a split mode option. How do I set the parameters to achieve the identical sensitivity, precision and accuracy?

[CE Instruments]

It is completely impossible to get IDENTICAL sensitivity, precision and accuracy.
Start by calculating the actual volume transferred and match the incubation conditions and start from there.