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- Posts: 22
- Joined: Fri Jan 31, 2014 7:19 pm
I was shown basics and over time have come close to getting clear separation of my target. I have found by my analytical machine that what I thought should be a clean fraction from my prep was not. Injecting water samples has eluted peaks which I thought my "built in cleaning" method would take care of.
They're both manual injectors and while I was never told details about when to close them back up I've rationalized that a higher %B than initial conditions shouldn't be allowed to enter. I only provide this as an example because I pretty much need an overhaul in technique which I am not getting from my peers. I would like to post and talk about my chromatagrams but I feel there is a lot of noobie stuff I need to go over before hand.
Where do I go/look? I've done my basic rounds of websites like the UCDavis ChemWiki but I'm still left wanting.
They're both manual injectors and while I was never told details about when to close them back up I've rationalized that a higher %B than initial conditions shouldn't be allowed to enter. I only provide this as an example because I pretty much need an overhaul in technique which I am not getting from my peers. I would like to post and talk about my chromatagrams but I feel there is a lot of noobie stuff I need to go over before hand.
Where do I go/look? I've done my basic rounds of websites like the UCDavis ChemWiki but I'm still left wanting.
