-
- Posts: 3
- Joined: Tue Nov 03, 2015 3:48 am
What to do when phosphate peak getting broad and small?
We used around 0.1-0.4ppm as standard 1,2 and 3 respectively.
The recovery for std 1 and 2 are not good. Thus affect the Coeff. Of determination of phosphate.
But there is no problem with micropipette.
We control our Coeff. Of Det. 99.5% above.
We also control the slope and fixed the offset to zero.
From our observation the Coeff.Det. and slope getting decreases and the peak look broad and small (standard 2 & 3). We want high and sharp peak.
We already used new suppressor.
But after use it for 3 weeks, the problem occurs for phosphate only.
Other ions are within control except phosphate.
What should we do?
Thanks.