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Retention Time Problem
Discussions about IC and related topics
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I am using DX100 IC, during my mdl run the analytes elutes ealier than expected. The flow rate is constant @ 2.0ml/min. What are the possible sources of retention time shift of anions (Cl,F, Br, No3,, NO2, SO4 and PO4). and what are the possible troubleshooting procedure. Thank you in advance.;
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- Posts: 28
- Joined: Fri May 14, 2010 2:53 pm
- Location: United Kingdom
Hello darylm,
Have you checked the composition of the eluent, the condition of the guard and analytical columns, and the column and detector temperatures. Any slight changes to any of these parameters may create a shift in retention time. In addition, If you are performing manual injections, have there been any changes to your injection technique. If you are using an autosampler, have the settings been altered.
Have you checked the composition of the eluent, the condition of the guard and analytical columns, and the column and detector temperatures. Any slight changes to any of these parameters may create a shift in retention time. In addition, If you are performing manual injections, have there been any changes to your injection technique. If you are using an autosampler, have the settings been altered.
Kind regards,
Ade Kujore
Marketing
Cecil Instruments
Cambridge
United Kingdom
email:- ade.kujore@cecilinstruments.com
telephone:- +44 (0) 1223 420821
web site:- www.cecilinstruments.com
Registered Number 909536
Ade Kujore
Marketing
Cecil Instruments
Cambridge
United Kingdom
email:- ade.kujore@cecilinstruments.com
telephone:- +44 (0) 1223 420821
web site:- www.cecilinstruments.com
Registered Number 909536
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