Debate at work regarding Cal standards
Posted: Thu Jun 12, 2014 6:24 pm
Hi Chromatography community. I am requesting some help in deciding a debate we are having at work regarding calibration curves and standards for standard Anions (F, Cl, NO2, NO3, Br, PO4, and SO4).
The debate is whether a blank or Zero point should be run as calibration standard one. The way things have always been is to run a blank as calibration standard 1 and then follow with our normal standards. With the purchase of some new instrumentation, the company has said a zero point is not necessary, and not a good practice to do. The methods we run are EPA 9056 and 300.0. The way the methods are written leaves the argument open for debate. I am wondering what the community here thinks.
The debate is whether a blank or Zero point should be run as calibration standard one. The way things have always been is to run a blank as calibration standard 1 and then follow with our normal standards. With the purchase of some new instrumentation, the company has said a zero point is not necessary, and not a good practice to do. The methods we run are EPA 9056 and 300.0. The way the methods are written leaves the argument open for debate. I am wondering what the community here thinks.