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- Posts: 94
- Joined: Wed May 22, 2019 5:19 pm
After the ex-boss left I looked and saw how she did it. Instead if updating retention times with a new column she manually assigned the peaks. Then afterwards she updated the retention times. Somehow that allowed the instrument to ignore the programmed integration parameters for the calibrators. I brought this up in the morning meeting and said I could not sign off on the data unless it was reprocessed. My ex-boss was not happy. Someone else said to her that I knew more about the instrument than her and she said 'I disagree." The chief finally came down on my side and told the ex-boss to reprocess the run.
Then late in the afternoon I was reviewing some data at my desk and the ex-boss comes over and asks when I'm leaving. I said 'In a few minutes.' Then she gave me a nasty glare and said "Because I'm not leaving until you leave." I said I would in a few and after she went away I left. I still have not seen any raw data she has generated. I looked in our data management system and see some results that have a failed sulfate spike, so I suspect some integration parameters are still wrong. With a new column and a low level sulfate it should not fail a spike.