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Siloxane analysis by Thermal Desorption GC-MS

Posted: Wed Jan 31, 2018 11:53 am
by noelcasey@gmail.com
Hello,

I am looking for forum advice on the optimum operating conditions for trace siloxane analysis by Thermal Desorption GC-MS while minimizing the problems of memory effects.

Instrumentation
Gerstel TDS 2 with tenax filled tube
CIS 4 cryo-cooled injector with tenax ta liner
Agilent 6890n GC, 5975C

Any advice would be greatly appreciated on this challenging analysis.

Best,

Noel Casey