-
- Posts: 102
- Joined: Tue Oct 06, 2020 10:01 pm
- Location: Australia
I'm assuming it's flying out too fast for me to catch. Conditions are:
DB-624, helium, Agilent 6890A/5975, inlet temp 150 deg. C
Hold at 28 deg. C for 10 mins (can't get the oven any cooler than that), then heat up to 250 deg. C for a couple min (to purge out anything left over).
Scanning 30-200 m/z
For reference, pentafluoroethane comes out at around 1.5 mins. So no idea how I'm going to see difluoromethane with that setup...
Any suggestions as to something I can knock together in the next 24 hours?