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- Posts: 7
- Joined: Fri Mar 24, 2017 1:27 am
I am having issues with the temperature of my GC-microECD.
Since It started to report signals of 2000 to 2500 Hz I performed a bake-out, but the detector can´t reach 400 °C.
It stays at 350 °C and after approximately 8 hours, gets to a maximum of 370 °C until the time of bake-out is reached.
Unfortunately the signal doesn´t get low, staying at 1900 Hz.
So i was wondering that maybe I need more time of bake-out. (The usual time I use is 28 to 30 hours) or there´s something wrong with the detector, i mean it can´t get to 400 °C.
The regular temperature for my method is 325°C.
I hope you guys can help me out
thanks for your time