7697A on Empower 3 - Instrument Failure
Posted: Thu Dec 21, 2017 10:13 am
Hi ,
Anybody came across this problem ?
Using the same instrument method ::
I set up a sample set using wizard and calibrate at the beginning (bracketing stds)
The headspace picks up vial, moves to oven then instrument failure occurs and HS vial
I removed the calibrate function from the sample set and it carried out vial preparation as normal and acquired data once injected
Any thoughts why it should fail with calibrate/quantitate commands ?
Anybody came across this problem ?
Using the same instrument method ::
I set up a sample set using wizard and calibrate at the beginning (bracketing stds)
The headspace picks up vial, moves to oven then instrument failure occurs and HS vial
I removed the calibrate function from the sample set and it carried out vial preparation as normal and acquired data once injected
Any thoughts why it should fail with calibrate/quantitate commands ?