7697A on Empower 3 - Instrument Failure

Discussions about GC and other "gas phase" separation techniques.

2 posts Page 1 of 1
Hi ,

Anybody came across this problem ?

Using the same instrument method ::

I set up a sample set using wizard and calibrate at the beginning (bracketing stds)
The headspace picks up vial, moves to oven then instrument failure occurs and HS vial

I removed the calibrate function from the sample set and it carried out vial preparation as normal and acquired data once injected

Any thoughts why it should fail with calibrate/quantitate commands ?

Anybody any thoughts on this

Carried out a sample set no problem without functions

when functions added as per sample set wizard 7697A errors with instrument failure

So adding functions after sampel set ran only option?

2 posts Page 1 of 1

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