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- Posts: 11
- Joined: Wed Sep 01, 2004 5:52 am
sample: 0,1 g methanol in 100ml ethanol
column : HP innowax 15 m 0,25 mm film ticknes 1 micrometer
flow: 3
inlet preassure 1,2 psi
split 30:1
inlet temp: 250 dC
detect temp: 250 dC
manual inject: 1 microlitr
I want to say that I use three difrent syringe I don't have leek in my equipment I change septa and ofcourse liner. I tray to decrising inlet temperature but without possitive effect .