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- Joined: Wed Apr 20, 2011 11:19 am
Following more details:
Column: SE 54; Carrier gas: helium; Injector: 320°c; Detector:320°c; oven:300°isotherm (50min)
Internal standard (IS): 0,5 % Octacosan
Standardsolution: 60mg tocopherol/5ml (THF) and 1ml of standard+1ml IS/5ml THF.
Sample preparation: 10 capsules +10 ml IS/50 ml THF.