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- Posts: 16
- Joined: Wed Aug 17, 2022 4:04 am
I am developing a HS-SPME GC-MS method for smoke taint. I can get a linear/repeatable cal curve for o/m/p- cresol, Guaicol, 4Me-Guaicol, 4Me Syringol but syringol doesn't show a linear peak as at lower conc (2ug/L) I can't accurately quantitate it (high bp). I can't find anything literature for HS-SPME of this compound (only LLE). There is a Thermo application but it has not been optimized for syringol ( it uses 80C extraction temp!!)
I really appreciate if anyone who has any experience.
Thanks in advance for your help.