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High RSD

Posted: Thu Jan 26, 2023 4:30 pm
by arv
Hello,
I've been finding high values for RSD when determining precision in our HS-GC. I prepped a 0.5% solution of ethanol.

Re: High RSD using HS-GC

Posted: Mon Jan 30, 2023 12:58 pm
by redjamesg
Have you tried stabilizing the headspace by adding a tiny amount of NaCl ?

Re: High RSD

Posted: Thu Feb 09, 2023 8:58 pm
by Peter Apps
Welcome to the forum.

You are new here, your first lesson is that sensible answers require actual questions, and nobody can troubleshoot without details of what you are doing and how.

Rod's law; the more you don't tell us the more we can't help you.

Peter

Re: High RSD

Posted: Tue Dec 19, 2023 9:28 am
by gyrusaudit
Did you add a tiny amount of NaCl? Have you finished the chemical analysis?
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