sodium sulfate cleaning
Posted: Wed Jul 01, 2020 5:33 pm
The EPA solid waste methods (3550C for example), say you should purify sodium sulfate by heating in a shallow tray at 400C for four hours, or cleaning it with DCM.
I've got a tiny little muffle furnace to work with, so unless I get real creative about how I interpret "shallow tray" (250ml beaker filled to the top? ) it's hard to clean enough - and we only use a couple hundred grams a day.
Anyone have a better way to do this that doesn't require dropping thousands on an oven just for this purpose? I haven't really figured out a good way to clean it with DCM that doesn't waste tons of solvent.
I did consider taking the column out of one of my GCs and using it as the oven...
I've got a tiny little muffle furnace to work with, so unless I get real creative about how I interpret "shallow tray" (250ml beaker filled to the top? ) it's hard to clean enough - and we only use a couple hundred grams a day.
Anyone have a better way to do this that doesn't require dropping thousands on an oven just for this purpose? I haven't really figured out a good way to clean it with DCM that doesn't waste tons of solvent.
I did consider taking the column out of one of my GCs and using it as the oven...