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- Posts: 2
- Joined: Thu Oct 01, 2015 12:13 pm
I´m brand new using gc ms. The equipment was shutted down for 1 year, and now we have to use it to proccess some wine samples using head space. The problem is that when I run auto tuning, my base peak is 28 or 14, and the 69 peak NEVER was twice the size of 28 peak. I looked for leaks and I can´t no detect any. I tried to fill the PFTBA with more sample and the capillary of that septum broked, is that important? any help will be great!!!!!!
Thanks,
Victoria