-
- Posts: 30
- Joined: Sat Sep 25, 2010 5:17 pm
I am experiencing issues on an Agilent 7890 GC-FID and hoped for some insight before digging into the split vent line and trap.
Conditions:
split/splitless inlet running in split mode
column flow 4 ml/min
split ratio 5
split flow 20 ml/min
total flow 27 ml/min
When the method is initialized or "set up" in Empower and the instrument tries to go to the set points, in order to reach the 20 ml/min split flow set point, the column flow jumps to around 8 ml/min. If the column flow is manually set to the correct 4 ml/min column flow on the GC keypad, it drops the split flow to 6 ml/min.
No leaks could be identified using electronic leak detector. I have narrowed down the issue in my mind to restriction in the split vent line or restriction in the split trap, but I wanted to get some input before I changed these out because they are a pain in the *ss to get to. I am hoping something more sinister isn't at work here like a malfunctioning EPC.
Any recommendations appreciated as always.
Regards,
Mike