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- Posts: 9
- Joined: Mon Nov 21, 2011 5:37 pm
I have a Varian 3800 with PFPD, I have set all parameters for the sulfur in gas analyses as per ASTM 6228, the problem is that I am trying to get the instrument to stabilize before the run and while watching the PFPD signal it is never stable,
So the PFPD signal is fluctuating before the run jumping from -2 to 2 and I remember it was very table and fluctuating in the range 0.005 up or down,
When I start the instrument anyway, the run is very noisy with noise up to 1000,
The square root is off,