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- Posts: 3
- Joined: Fri Mar 27, 2015 6:55 pm
But, when iam injecting a number of samples (eg 10 samples), in that case 4 to 5 "blank injections" are needed and i can't give guarantee to pass the bracketing standard. This API is soluble in THF and MDC. My diluent is 0.1%OPA and Acetonitrile(50:50). It is not soluble in methanol, ACN and water (mixtures of these solvents) as such. Please suggest me, how to solve this problem?