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- Posts: 1
- Joined: Fri Jul 31, 2015 9:25 pm
Powers above me are saying that the data can be saved IF, to support the increased injection volume they would like the CTL to include the calibration parameters for their HPLC, specifically the injection loop. If the increased volume still falls within their calibration parameters, that coupled with the standards being injected at the same level and passing system suitability, the validity of the run can be supported.
I assumed this was a cut and dry issue... if the wrong injection volume is used, the data is invalidated with a very clear assignable cause. The samples and standards are injected again using the proper injection volume. Is this not the case?